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Continuous Flow Chlorination of Alkenyl Iodides Promoted by Copper Tubing
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A simple continuous flow synthesis of alkenyl chlorides from the corresponding readily available alkenyl iodides in copper reactor tubing is described. A variety of alkenyl chlorides were obtained in good to excellent yields with full retention of the double bond geometry. The reaction time was reduced by a factor of 24–48 compared to the batch process.
Georg Thieme Verlag KG
Title: Continuous Flow Chlorination of Alkenyl Iodides Promoted by Copper Tubing
Description:
A simple continuous flow synthesis of alkenyl chlorides from the corresponding readily available alkenyl iodides in copper reactor tubing is described.
A variety of alkenyl chlorides were obtained in good to excellent yields with full retention of the double bond geometry.
The reaction time was reduced by a factor of 24–48 compared to the batch process.
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