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Preparation of A Trifluoromethyl Transfer Agent: 1‐Trifluoromethyl‐1,3‐Dihydro‐3,3‐Dimethyl‐1,2‐Benziodoxole
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Abstract
2‐(2‐Iodophenyl)propan‐2‐ol
1‐Chloro‐1,3‐dihydro‐3,3‐dimethyl‐1,2‐benziodoxole
1‐Trifluoromethyl‐1,3‐dihydro‐3,3‐dimethyl‐1,2‐benziodoxole
Iodomethane
Methyl 2‐iodobenzoate
Tert
‐butyl hypochlorite
(Trifluoromethyl)trimethylsilane
Tetrabutylammonium difluorotriphenylsilicate(IV)
2‐Iodobenzoic acid
Sodium (meta)periodate
1‐Hydroxy‐1,2‐benziodoxol‐3‐(1
H
)‐one
Acetic anhydride
1‐Acetoxy‐1,2‐benziodoxol‐3‐(1
H
)‐one
Cesium fluoride
1‐(Trifluoromethyl)‐1,2‐benziodoxol‐3(1
H
)‐one
Ethyl (
R
)‐2‐amino‐3‐mercaptopropanoate hydrochloride
Title: Preparation of
A
Trifluoromethyl Transfer Agent: 1‐Trifluoromethyl‐1,3‐Dihydro‐3,3‐Dimethyl‐1,2‐Benziodoxole
Description:
Abstract
2‐(2‐Iodophenyl)propan‐2‐ol
1‐Chloro‐1,3‐dihydro‐3,3‐dimethyl‐1,2‐benziodoxole
1‐Trifluoromethyl‐1,3‐dihydro‐3,3‐dimethyl‐1,2‐benziodoxole
Iodomethane
Methyl 2‐iodobenzoate
Tert
‐butyl hypochlorite
(Trifluoromethyl)trimethylsilane
Tetrabutylammonium difluorotriphenylsilicate(IV)
2‐Iodobenzoic acid
Sodium (meta)periodate
1‐Hydroxy‐1,2‐benziodoxol‐3‐(1
H
)‐one
Acetic anhydride
1‐Acetoxy‐1,2‐benziodoxol‐3‐(1
H
)‐one
Cesium fluoride
1‐(Trifluoromethyl)‐1,2‐benziodoxol‐3(1
H
)‐one
Ethyl (
R
)‐2‐amino‐3‐mercaptopropanoate hydrochloride.
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