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Synthesis of perfume compound etil p-anisat from anethole
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Synthesis of ethyl p-anisate from anethole has been done. Ethyl p-anisate is ester compound which can use as perfume component. p-anisic acid was synthesized from anethole (1 mole) which oxidised by KMnO4 (3 moles) at 40oC for 2 hours. Esterification with ethanol carried out at 78,5oC for 6 hours. Identification and determination structure compound of product synthesis used spectroscopic methods (GC, GC-MS and IR). Anethole has been isolated from anise oil as 90,3%. p-Anisic acid and ethyl p-anisate as synthesized products got 45% and 79,9% respectively.
Title: Synthesis of perfume compound etil p-anisat from anethole
Description:
Synthesis of ethyl p-anisate from anethole has been done.
Ethyl p-anisate is ester compound which can use as perfume component.
p-anisic acid was synthesized from anethole (1 mole) which oxidised by KMnO4 (3 moles) at 40oC for 2 hours.
Esterification with ethanol carried out at 78,5oC for 6 hours.
Identification and determination structure compound of product synthesis used spectroscopic methods (GC, GC-MS and IR).
Anethole has been isolated from anise oil as 90,3%.
p-Anisic acid and ethyl p-anisate as synthesized products got 45% and 79,9% respectively.
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